ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

Base Information

Chemical Name:ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate
CAS No.:699015-63-9
Molecular Formula:C₃₀H₃₃ClN₂O₇S
Molecular Weight:601.12
Hs Code.:

Synonyms:ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

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Chemical Property of ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

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Technology Process of ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

There total 2 articles about ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 699015-61-7
tert-Butyl [(2R)-2-(3-chlorophenyl)-2-hydroxyethyl][2-[4-[(triisopropylsilyl)thio]phenyl]ethyl]carbamate

: 320-98-9
5-fluoro-2-nitrobenzoic acid

: 699015-63-9
ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

Guidance literature:: tert-Butyl [(2R)-2-(3-chlorophenyl)-2-hydroxyethyl][2-[4-[(triisopropylsilyl)thio]phenyl]ethyl]carbamate; 5-fluoro-2-nitrobenzoic acid; With potassium carbonate; cesium fluoride; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 1.5h;

With ethyl iodide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 72h;

Reference yield:

: 699015-61-7
tert-Butyl [(2R)-2-(3-chlorophenyl)-2-hydroxyethyl][2-[4-[(triisopropylsilyl)thio]phenyl]ethyl]carbamate

: 320-98-9
5-fluoro-2-nitrobenzoic acid

: 75-03-6
ethyl iodide

: 699015-63-9
ethyl 5-[[4-[2-[(tert-butoxycarbonyl)[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]-amino]ethyl]phenyl]thio]-2-nitrobenzoate

Guidance literature:: tert-Butyl [(2R)-2-(3-chlorophenyl)-2-hydroxyethyl][2-[4-[(triisopropylsilyl)thio]phenyl]ethyl]carbamate; 5-fluoro-2-nitrobenzoic acid; With potassium carbonate; cesium fluoride; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 1.5h;

ethyl iodide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 72h;