1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Base Information

Chemical Name:1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide
CAS No.:1620644-73-6
Molecular Formula:C₂₄H₂₃BrNO₃*I
Molecular Weight:580.26
Hs Code.:

Synonyms:1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

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Chemical Property of 1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

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Technology Process of 1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

There total 9 articles about 1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1620646-00-5
2-(3-bromopyridin-4-yl)methyl-5,6-dimethoxy-2,3-dihydro-1H-inden-1-one

: 100-39-0
benzyl bromide

: 1620644-73-6
1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Guidance literature:: With sodium iodide; In dichloromethane; for 18h; Reflux;

Reference yield:

: 53295-44-6
5,6-(dimethoxy)-2-(ethoxycarbonyl)-indan-1-one

: 1620644-73-6
1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; sodium iodide / acetone / 6 h / Reflux

2: water; potassium hydroxide / ethanol / 0.5 h / Reflux

3: sodium iodide / dichloromethane / 18 h / Reflux

With water; potassium carbonate; sodium iodide; potassium hydroxide; In ethanol; dichloromethane; acetone;

Reference yield:

: 1620645-98-8
ethyl 2-((3-bromopyridin-4-yl)methyl)-5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

: 1620644-73-6
1-benzyl-3-bromo-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: water; potassium hydroxide / ethanol / 0.5 h / Reflux

2: sodium iodide / dichloromethane / 18 h / Reflux

With water; sodium iodide; potassium hydroxide; In ethanol; dichloromethane;