(2-naphthyl)triphenylstannane

Base Information

Chemical Name:(2-naphthyl)triphenylstannane
CAS No.:274928-10-8
Molecular Formula:C₂₈H₂₂Sn
Molecular Weight:477.193
Hs Code.:

Synonyms:(2-naphthyl)triphenylstannane

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Chemical Property of (2-naphthyl)triphenylstannane

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Technology Process of (2-naphthyl)triphenylstannane

There total 2 articles about (2-naphthyl)triphenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 16519-26-9
diethyl naphthalen-2-yl phosphate

: sodium triphenylstannide

: 274928-10-8
(2-naphthyl)triphenylstannane

Guidance literature:: With sodium; In ammonia; Irradiation (UV/VIS); react. Ph3SnNa with 2-C10H7OPO(OEt)2 in liquid ammonia in the presence of Na metal under UV irradiation for 6 h; yield was determined by GC;
DOI:10.1021/om000013l

Reference yield: 100.0%

: 16519-26-9
diethyl naphthalen-2-yl phosphate

: 639-58-7
triphenyltin chloride

: 274928-10-8
(2-naphthyl)triphenylstannane

Guidance literature:: With sodium; In ammonia; Irradiation (UV/VIS); (C6H5)3SnCl was dissolved in ammonia, Na metal was added until a blue color persisted for 5 min, when the blue color dissapeared, phosphate ester was added, the mixt. was UV-irradiated with stirring for 4 h; excess of CH3I was added, NH3 was evapd., the residue was treated with water, extd. with ether, washed with aq. satd. soln. of NaCl, dried over MgSO4, recrystd. in ethanol;
DOI:10.1021/om010878e