methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Base Information

• Chemical Name: methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate
• CAS No.: 1369803-32-6
• Molecular Formula: C₁₈H₁₈N₄O₅S
• Molecular Weight: 402.431

Synonyms:methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Chemical Property of methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Chemical Property:

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Technology Process of methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

There total 6 articles about methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-[(4-nitrophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate (1369803-58-6) → methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate (1369803-32-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 5h;

Reference yield:

methyl ({4-[(tert-butoxycarbonyl)amino]phenyl}sulfonyl)-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate → methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate (1369803-32-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

methyl 2-({4-[(tert-butoxycarbonyl)amino]phenyl}sulfonyl)-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate (1369803-31-5) → methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate (1369803-32-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;

upstream raw materials:

methyl 2-[(4-nitrophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

methyl 2-({4-[(tert-butoxycarbonyl)amino]phenyl}sulfonyl)-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

methyl [(4-aminophenyl)sulfanyl]acetate

methyl ({4-[(tert-butoxycarbonyl)amino]phenyl}sulfanyl)acetate

Downstream raw materials:

2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

methyl 2-[(4-{[(4-fluorophenyl)carbamoyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

2-[(4-{[(4-fluorophenyl)carbamoyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoic acid

methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

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