methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Base Information

Chemical Name:methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate
CAS No.:1369803-68-8
Molecular Formula:C₂₅H₂₁FN₄O₆S
Molecular Weight:524.529
Hs Code.:

Synonyms:methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

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Chemical Property of methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

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Technology Process of methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

There total 6 articles about methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369803-32-6
methyl 2-[(4-aminophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

: 1711-07-5
3-fluorobenzoyl chloride

: 1369803-68-8
methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 1369803-58-6
methyl 2-[(4-nitrophenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

: 1369803-68-8
methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 5 h

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1369803-31-5
methyl 2-({4-[(tert-butoxycarbonyl)amino]phenyl}sulfonyl)-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

: 1369803-68-8
methyl 2-[(4-{[(3-fluorophenyl)carbonyl]amino}phenyl)sulfonyl]-4-(4-oxo-1,2,3-benzotriazin-3(4H)-yl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;