9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

Base Information

Chemical Name:9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine
CAS No.:583047-64-7
Molecular Formula:C₃₁H₃₈N₆O₆Si
Molecular Weight:618.765
Hs Code.:

Synonyms:9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

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Chemical Property of 9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

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Technology Process of 9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

There total 8 articles about 9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₆N₆O₆Si

: 583047-64-7
9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 0.5h;
DOI:10.1081/NCN-120037508

Reference yield:

: 583047-61-4
9-(2-deoxy-ribo-pentofuranosyl)-2,6-dibenzamidopurine

: 583047-64-7
9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 3 h / 20 °C

2: imidazole / dimethylformamide / 20 °C

3: 28.8 g / p-toluenesulfonic acid hydrate / CHCl₃; methanol / 0.25 h / 0 °C

4: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; pyridine; trifluoroacetic acid / toluene; dimethylsulfoxide / 2 h / 20 °C

5: NaOH / dioxane; H₂O / 3 h / 20 °C

6: 30.83 g / NaBH₄ / ethanol / 0.5 h / 0 °C

With pyridine; 1H-imidazole; sodium hydroxide; sodium tetrahydroborate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In 1,4-dioxane; methanol; ethanol; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 4: Moffatt oxidation;
DOI:10.1081/NCN-120037508

Reference yield:

: C₃₀H₃₄N₆O₅Si

: 583047-64-7
9-(3-O-tert-butyldimethylsilyl-2-deoxy-4-C-hydroxymethyl-ribo-pentofuranosyl)-2,6-dibenzamidopurine

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / dioxane; H₂O / 3 h / 20 °C

2: 30.83 g / NaBH₄ / ethanol / 0.5 h / 0 °C

With sodium hydroxide; sodium tetrahydroborate; In 1,4-dioxane; ethanol; water;
DOI:10.1081/NCN-120037508