(E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

Base Information

Chemical Name:(E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate
CAS No.:1396630-44-6
Molecular Formula:C₁₉H₁₉F₃N₂O₄S
Molecular Weight:428.432
Hs Code.:

Synonyms:(E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

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Chemical Property of (E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

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Technology Process of (E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

There total 4 articles about (E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1334682-29-9
trifluoromethanesulfonic acid 2-(4-methyl-2-oxo-pentanoylamino)phenyl ester

: 62-53-3
aniline

: 1396630-44-6
(E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

Guidance literature:: With trifluoroacetic acid; In toluene; at 20 ℃; Molecular sieve; Inert atmosphere; Sealed tube;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j

Reference yield:

: 132993-22-7
2-nitrophenyl trifluoromethanesulfonate

: 1396630-44-6
(E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: iron; acetic acid / ethanol / 5 h / Reflux; Inert atmosphere

2: dicyclohexyl-carbodiimide / chloroform / 3 h / 0 °C / Inert atmosphere

3: trifluoroacetic acid / toluene / 20 °C / Molecular sieve; Inert atmosphere; Sealed tube

With iron; acetic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid; In ethanol; chloroform; toluene;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j

Reference yield:

: 38164-55-5
2-(aminophenyl)trifluoromethanesulfonate

: 1396630-44-6
(E)-2-(4-methyl-2-(phenylimino)pentanamido)phenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / chloroform / 3 h / 0 °C / Inert atmosphere

2: trifluoroacetic acid / toluene / 20 °C / Molecular sieve; Inert atmosphere; Sealed tube

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In chloroform; toluene;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j