N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL

Base Information

Chemical Name:N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL
CAS No.:154875-87-3
Molecular Formula:C₁₀H₉ClF₃N
Molecular Weight:235.636
Hs Code.:
Mol file:154875-87-3.mol

Synonyms:N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL

Suppliers and Price of N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL

Chemical Property:

Boiling Point:54-55 °C(Press: 9 Torr)
PKA:-1.89±0.50(Predicted)
Density:1.22±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:

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Technology Process of N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL

There total 1 articles about N-(2-ETHYLPHENYL)-2,2,2-TRIFLUOROACETIMIDOYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 578-54-1
ortho-ethylaniline

: 76-05-1
trifluoroacetic acid

: 154875-87-3
N-(2-ethylphenyl)-2,2,2-trifluoroacetimidoyl chloride

Guidance literature:: With tetrachloromethane; triethylamine; triphenylphosphine; for 3h; Heating;
DOI:10.1055/s-2007-967950

Reference yield:

: 154875-87-3
N-(2-ethylphenyl)-2,2,2-trifluoroacetimidoyl chloride

: 132502-93-3
2-trifluoromethyl-indole-3-acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / N-bromosuccinimide; benzoyl peroxide / CCl₄ / Heating

2: 82 percent / magnesium / tetrahydrofuran / 2 h / 0 °C

3: 93 percent / NaH; Me₂SO / various solvent(s); tetrahydrofuran / 2 h / 20 °C

4: 85 percent / N-bromosuccinimide; 2,2'-azobisisobutyronitrile / CCl₄ / 5 h / Heating

5: 94 percent / NaCN / ethanol / 6 h / 20 °C

6: 62 percent / aq. AcOH; aq. HCl / 336000 h / Heating

With hydrogenchloride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium cyanide; sodium hydride; magnesium; acetic acid; dimethyl sulfoxide; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; ethanol; 2: Grignard cyclization reaction;
DOI:10.1016/j.jfluchem.2007.04.023