1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

Base Information

Chemical Name:1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose
CAS No.:124780-59-2
Molecular Formula:C₃₄H₄₀N₂O₇
Molecular Weight:588.701
Hs Code.:

Synonyms:1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

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Chemical Property of 1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

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Technology Process of 1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

There total 7 articles about 1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124780-57-0
Methyl 2,3,4-Tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranoside

: 108-24-7
acetic anhydride

: 124780-59-2
1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

Guidance literature:: With sulfuric acid; at -20 - 0 ℃;
DOI:10.1021/jo00292a044

Reference yield: 100.0%

: 124915-83-9
Methyl 2,3,4-Tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-1-thio-D-erythro-β-D-galacto-octopyranoside

: 108-24-7
acetic anhydride

: 124780-59-2
1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

Guidance literature:: With sulfuric acid; at -20 - 0 ℃;
DOI:10.1021/jo00292a044

Reference yield:

: 124780-66-1
methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

: 124780-59-2
1-O-Acetyl-2,3,4-tris-O-(phenylmethyl)-6,8-dideoxy-7,6-<2-(N,N-dimethylamino)-1-oxa-3-azaprop-2-eno>-D-erythro-α-D-galacto-octopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / Ambient temperature

3: imidazole, NaH / dimethylformamide / 1) 12h, 0 deg C, 2) 48h, r.t.

4: 100 percent / NaH / dimethylformamide / 12 h / Ambient temperature

5: 100 percent / sulfuric acid / -20 - 0 °C

With pyridine; 1H-imidazole; sulfuric acid; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00292a044