methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

Base Information

Chemical Name:methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside
CAS No.:124780-66-1
Molecular Formula:C₂₃H₂₈O₅
Molecular Weight:384.472
Hs Code.:

Synonyms:methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

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Technology Process of methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

There total 17 articles about methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 131529-70-9
methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-4-O-(4-methoxybenzyl)-α-D-galacto-oct-6-enoside

: 124780-66-1
methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

Guidance literature:: With ammonium cerium(IV) nitrate; In water; acetonitrile; for 3h;
DOI:10.1071/CH9901643

Reference yield:

: 124780-53-6
(3aS,4R,6S,7R,7aS)-7-Benzyloxy-6-methoxy-2,2-dimethyl-4-((E)-propenyl)-tetrahydro-[1,3]dioxolo[4,5-c]pyran

: 100-39-0
benzyl bromide

: 124780-66-1
methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; di(n-butyl)tin oxide; In benzene; Heating;
DOI:10.1021/jo00292a044

Reference yield:

: 130523-98-7
(2S,3S,4S,5R,6S)-4,5-Bis-benzyloxy-6-methoxy-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-carbaldehyde

: 124780-66-1
methyl (E)-2,3-di-O-benzyl-6,7,8-trideoxy-α-D-galacto-oct-6-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) THF, 0 deg C, 5 min, 2.) 30 min

2: 97 percent / cerium(IV) ammonium nitrate / acetonitrile; H₂O / 0.5 h

With n-butyllithium; ammonium cerium(IV) nitrate; In water; acetonitrile;
DOI:10.1071/CH9901643