cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

Base Information

Chemical Name:cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate
CAS No.:1174738-27-2
Molecular Formula:C₁₅H₂₀BrNO₃S
Molecular Weight:374.299
Hs Code.:

Synonyms:cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

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Chemical Property of cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

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Technology Process of cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

There total 2 articles about cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1073338-25-6
cis-3-piperidin-1-ylcyclobutanol

: 98-58-8
4-bromobenzenesulfonyl chloride

: 1174738-27-2
cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

Guidance literature:: With 1-methyl-1H-imidazole; In ethyl acetate; at 20 ℃; for 12h;

Reference yield:

: 110-89-4
piperidine

: 1174738-27-2
cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / 1,4-dioxane / 2.17 h / 20 °C

1.2: 0.33 h / 20 - 30 °C

2.1: sodium tetrahydroborate; ethanol / 50 °C

3.1: 1-methyl-1H-imidazole / ethyl acetate / 12 h / 20 °C

With 1-methyl-1H-imidazole; sodium tetrahydroborate; ethanol; trifluoroacetic acid; In 1,4-dioxane; ethyl acetate;

Reference yield: 99.0%

: 1174738-27-2
cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate

: 1074-36-8
4-mercaptobenzoic acid

: 1174737-87-1
4-{[trans-3-(piperidin-1-yl)cyclobutyl]sulfanyl}benzoic acid

Guidance literature:: 4-mercaptobenzoic acid; With sodium thiosulfate; In N,N-dimethyl-formamide; for 1h; Molecular sieve;

cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 - 50 ℃; for 14h;