Dimethyl Azidomalonate

Base Information

Chemical Name:Dimethyl Azidomalonate
CAS No.:68641-18-9
Molecular Formula:C₁₈H₁₇N₃O₅
Molecular Weight:355.35
Hs Code.:

Dimethyl Azido<p-(benzyloxy)phenyl>malonate

Synonyms:Dimethyl Azidomalonate

Suppliers and Price of Dimethyl Azidomalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl Azidomalonate

Chemical Property:

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Technology Process of Dimethyl Azidomalonate

There total 3 articles about Dimethyl Azidomalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68641-16-7
(4-benzyloxy-phenyl)-acetic acid methyl ester

: 68641-18-9
Dimethyl Azidomalonate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaH / diethyl ether; methanol / 24 h / Ambient temperature

2: 1.) NaH, HMPA, 2.) p-Toluenesulfonyl azide / 1.) THF, room temp., 2h, 2.) reflux, 2h

With N,N,N,N,N,N-hexamethylphosphoric triamide; 4-toluenesulfonyl azide; sodium hydride; In methanol; diethyl ether;
DOI:10.1021/jo00328a002

Reference yield:

: 68641-17-8
4-benzyloxyphenyl malonic acid dimethylester

: 68641-18-9
Dimethyl Azidomalonate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; 4-toluenesulfonyl azide; sodium hydride; Yield given. Multistep reaction; 1.) THF, room temp., 2h, 2.) reflux, 2h;
DOI:10.1021/jo00328a002