trans-1-phenylmethanimine triethylborane

Base Information Edit

Chemical Name:trans-1-phenylmethanimine triethylborane
CAS No.:273749-15-8
Molecular Formula:C₁₃H₂₂BN
Molecular Weight:203.135
Hs Code.:
Mol file:273749-15-8.mol

Synonyms:trans-1-phenylmethanimine triethylborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1-phenylmethanimine triethylborane Edit

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Technology Process of trans-1-phenylmethanimine triethylborane

There total 2 articles about trans-1-phenylmethanimine triethylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 97-94-9
triethyl borane

: 622-79-7
benzyl azide

: 273749-15-8
trans-1-phenylmethanimine triethylborane

Guidance literature:: With C₄₈H₄₈N₂O₄Ru₂; In tetrahydrofuran; hexane; at 20 ℃; for 10h; chemoselective reaction; Inert atmosphere; Irradiation;
DOI:10.1002/anie.201204483

Reference yield:

: 22560-16-3
lithium triethylborohydride

: 100-47-0
benzonitrile

: 273749-15-8
benzaldimine-triethylborane complex

Guidance literature:: lithium triethylborohydride; benzonitrile; In tetrahydrofuran; at 0 ℃; for 2h;

With methanol; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.3987/COM-10-S(E)95

Reference yield:

: 273749-15-8
benzaldimine-triethylborane complex

: (+)-B-allyldiisopinocampheylborane

: 4383-23-7,110216-57-4,115224-13-0,130608-03-6
(S)-1-phenylbut-3-en-1-amine

Guidance literature:: benzaldimine-triethylborane complex; (+)-B-allyldiisopinocampheylborane; With methanol; In tetrahydrofuran; at -78 ℃;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 25 ℃; for 12h; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.06.076