(3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Base Information

Chemical Name:(3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal
CAS No.:1204686-04-3
Molecular Formula:C₃₄H₄₆O₄Si
Molecular Weight:546.822
Hs Code.:

Synonyms:(3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

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Technology Process of (3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

There total 1 articles about (3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₅H₄₈O₄Si

: 1204686-04-3
(3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Guidance literature:: With hydrogenchloride; water; In ethyl acetate; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1218152

Reference yield: 80.0%

: 1204686-04-3
(3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1204685-98-2
tert-butyl[(2S,3S,5R,6S)-5-(4-methoxybenzyloxy)-3,6-dimethylnon-8-en-2-yloxy]diphenylsilane

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

(3S,4R,6S,7S)-7-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1218152