1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Base Information

Chemical Name:1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose
CAS No.:14233-58-0
Molecular Formula:C₄₅H₄₂O₅
Molecular Weight:662.825
Hs Code.:

Synonyms:1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Suppliers and Price of 1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

There total 3 articles about 1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 14233-55-7
2,3,5-tri-O-benzyl-1-O-trityl-D-arabinitol

: 14233-58-0
1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201601639

Reference yield:

: 14233-53-5
3,4,6-tri-O-benzyl-D-arabinitol

: 14233-58-0
1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Guidance literature:: Multi-step reaction with 2 steps

1: Py

2: DMSO, Ac₂O

With pyridine; acetic anhydride; dimethyl sulfoxide;
DOI:10.1021/jo01286a036

Reference yield:

: 89824-86-2
(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-methoxytetrahydrofuran

: 14233-58-0
1,3,4-tri-O-benzyl-5-O-trityl-D-threo-pentulose

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; sulfuric acid / water / 0.5 h / 100 °C / Inert atmosphere

2: sodium tetrahydroborate; ethanol / 5 h / 0 - 20 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 8 h / 20 °C / Inert atmosphere

4: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; ethanol; sulfuric acid; Dess-Martin periodane; acetic acid; triethylamine; In dichloromethane; water;
DOI:10.1002/ejoc.201601639