1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

Base Information

Chemical Name:1,3,4-tri-O-benzyl-D-erythro-pentulofuranose
CAS No.:14233-60-4
Molecular Formula:C₂₆H₂₈O₅
Molecular Weight:420.505
Hs Code.:

Synonyms:1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

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Chemical Property of 1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

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Technology Process of 1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

There total 11 articles about 1,3,4-tri-O-benzyl-D-erythro-pentulofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1,3,4-tri-O-benzyl-5-O-trityl-D-erythro-pentulose

: 14233-60-4
1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

Guidance literature:: With formic acid; In diethyl ether; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/ejoc.201601639

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 14233-60-4
1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / methanol

2: Py

3: DMSO, Ac₂O

4: aq. AcOH

With pyridine; sodium tetrahydroborate; acetic anhydride; acetic acid; dimethyl sulfoxide; In methanol;
DOI:10.1021/jo01286a036

Reference yield:

: 122565-72-4
2,3,5-tri-O-benzyl-D-lyxitol

: 14233-60-4
1,3,4-tri-O-benzyl-D-erythro-pentulofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; dmap / dichloromethane / 8 h / 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: formic acid / diethyl ether / 0.25 h / 20 °C / Inert atmosphere

With dmap; formic acid; Dess-Martin periodane; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1002/ejoc.201601639