Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

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Chemical Name:Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester
CAS No.:117490-60-5
Molecular Formula:C₂₉H₂₉N₃O₁₀
Molecular Weight:579.563
Hs Code.:

Synonyms:Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

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Chemical Property of Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

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Technology Process of Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

There total 10 articles about Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.3%

: 128858-15-1
8-benzyloxy-7,8-didemethyl-5-deazariboflavin 2',3',4'-triacetate 5'-trityl ether

: 117490-60-5
Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

Guidance literature:: With hydrogenchloride; In chloroform; at 0 ℃; for 1h;

Reference yield:

: 117490-58-1
8-benzyloxy-7,8-didemethyl-5-deazariboflavin

: 117490-60-5
Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 0 deg C to r.t.

2: pyridine / Ambient temperature

3: HCl (gas) / CHCl₃ / 0.5 h / 0 °C

With pyridine; hydrogenchloride; In chloroform;
DOI:10.1039/c39880000524

Reference yield:

: 8-Benzyloxy-10-((2S,3S,4R)-2,3,4-trihydroxy-5-trityloxy-pentyl)-10H-pyrimido[4,5-b]quinoline-2,4-dione

: 117490-60-5
Acetic acid (1S,2S,3R)-2,3-diacetoxy-1-(8-benzyloxy-2,4-dioxo-3,4-dihydro-2H-pyrimido[4,5-b]quinolin-10-ylmethyl)-4-hydroxy-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / Ambient temperature

2: HCl (gas) / CHCl₃ / 0.5 h / 0 °C

With pyridine; hydrogenchloride; In chloroform;
DOI:10.1039/c39880000524