1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

Base Information

Chemical Name:1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine
CAS No.:868835-90-9
Molecular Formula:C₂₅H₃₀N₂O₄
Molecular Weight:422.524
Hs Code.:

Synonyms:1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

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Chemical Property of 1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

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Technology Process of 1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

There total 5 articles about 1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 868835-90-9
1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

Guidance literature:

Reference yield:

: 66917-06-4
N-(4-azidobutyl)phthalimide

: 868835-90-9
1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂ / Pd/C / ethanol / 12 h / 1292.87 Torr

2.1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C

2.2: NaCNBH₃ / 1,2-dichloro-ethane; methanol / 12 h

3.1: aq. NaHCO₃; NaCl / CH₂Cl₂ / 12 h / Heating

With hydrogen; sodium hydrogencarbonate; acetic acid; sodium chloride; palladium on activated charcoal; In ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm0505009

Reference yield:

: 5394-18-3
2-(4-bromobutyl)isoindoline-1,3-dione

: 868835-90-9
1-N-[4-(methyl)benzyl]-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaN₃ / dimethylformamide / 5 h

2.1: H₂ / Pd/C / ethanol / 12 h / 1292.87 Torr

3.1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C

3.2: NaCNBH₃ / 1,2-dichloro-ethane; methanol / 12 h

4.1: aq. NaHCO₃; NaCl / CH₂Cl₂ / 12 h / Heating

With sodium azide; hydrogen; sodium hydrogencarbonate; acetic acid; sodium chloride; palladium on activated charcoal; In ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009