methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

Base Information

Chemical Name:methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate
CAS No.:1426530-73-5
Molecular Formula:C₁₇H₁₄BrN₃O₃
Molecular Weight:388.22
Hs Code.:

Synonyms:methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

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Chemical Property of methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

Chemical Property:

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Technology Process of methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

There total 3 articles about methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18595-18-1
3-amino-4-methyl benzoic acid methyl ester

: 1019021-93-2
7-bromoimidazol[1,2-a]pyridine-3-carboxylic acid

: 1426530-73-5
methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

Guidance literature:: 7-bromoimidazol[1,2-a]pyridine-3-carboxylic acid; With thionyl chloride; for 2h; Inert atmosphere; Reflux;

3-amino-4-methyl benzoic acid methyl ester; With pyridine; at 20 ℃; Inert atmosphere;

Reference yield:

: 1134327-98-2
7-bromoimidazo[1,2-a]pyridin-3-carboxylate ethyl ester

: 1426530-73-5
methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / methanol; water / 0.67 h / 60 °C

2.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

2.2: 20 °C / Inert atmosphere

With thionyl chloride; water; sodium hydroxide; In methanol; water;

Reference yield:

: 84249-14-9
2-amino-4-bromopyridine

: 1426530-73-5
methyl 3-(7-bromoimidazo[1,2-a]pyridine-3-carboxamido)-4-methylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / ethanol / 3 h / 90 °C

1.2: 18 h / 20 - 90 °C

2.1: water; sodium hydroxide / methanol; water / 0.67 h / 60 °C

3.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

3.2: 20 °C / Inert atmosphere

With thionyl chloride; sulfuric acid; water; sodium hydroxide; In methanol; ethanol; water;