2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:137297-51-9
Molecular Formula:C₁₅H₂₃BO₃
Molecular Weight:262.157
Hs Code.:
DSSTox Substance ID:DTXSID701165672
Nikkaji Number:J626.954K

Synonyms:137297-51-9;2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;2-(Benzyloxy)ethylboronic acid pinacol ester;4,4,5,5-tetramethyl-2-(2-phenylmethoxyethyl)-1,3,2-dioxaborolane;2-[2-(BENZYLOXY)ETHYL]-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE;Pinacol (benzyloxy)ethylboronate;DTXSID701165672;BS-30765;CS-0176796;EN300-1702774;Z2466490266;4,4,5,5-Tetramethyl-2-[2-(phenylmethoxy)ethyl]-1,3,2-dioxaborolane

Suppliers and Price of 2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:262.1740248
Heavy Atom Count:19
Complexity:269

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)CCOCC2=CC=CC=C2

Technology Process of 2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 4 articles about 2-(2-(Benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 13826-27-2
2,2'-bis(1,3,2-benzodioxaborole)

: 1462-37-9
bromoethyl-2-benzyl ether

: 137297-51-9
2-(2-(benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 2,2'-bis(1,3,2-benzodioxaborole); bromoethyl-2-benzyl ether; With p-phenylpyridine; sodium methylate; In acetonitrile; for 24h; Glovebox; Irradiation; Sealed tube; Inert atmosphere;

2,3-dimethyl-2,3-butane diol; With triethylamine; In acetonitrile; for 1h; Glovebox; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201912564

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: C₉H₁₇B₆O^(1-)*C₁₆H₃₆N⁽¹⁺⁾

: 137297-51-9
2-(2-(benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With magnesium sulfate; 7,7',8,8'-tetracyanoquinodimethane; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.chempr.2019.07.018

Reference yield:

: 1462-37-9
bromoethyl-2-benzyl ether

: 73183-34-3
bis(pinacol)diborane

: 137297-51-9
2-(2-(benzyloxy)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With copper(l) iodide; lithium methanolate; In N,N-dimethyl-formamide; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jo3021665