phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate

Base Information

• Chemical Name: phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate
• CAS No.: 1315128-03-0
• Molecular Formula: C₁₉H₂₉NO₄Si
• Molecular Weight: 363.529

Synonyms:phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate

Chemical Property of phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate

Chemical Property:

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Technology Process of phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate

There total 2 articles about phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C12H24O4Si + benzyl formylcarbamate (69261-49-0) → (-)-phenylmethyl [(1R)-1-({[(1,1-dimethylethyl)(dimethyl)silyl]oxy}methyl)prop-2-en-1-yl]formylcarbamate (1315128-01-8) + phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate (1315128-03-0)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 20 ℃; for 3h; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201100649

Reference yield:

C12H24O4Si + benzyl formylcarbamate (69261-49-0) → phenylmethyl [(1S)-1-({[(1,1-dimethylethyl)(dimethyl)silyl]oxy}methyl)prop-2-en-1-yl]formylcarbamate (1315128-81-4) + phenylmethyl ((2E)-4-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}but-2-en-1-yl)formylcarbamate (1315128-03-0)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 20 ℃; for 3h; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201100649

upstream raw materials:

benzyl formylcarbamate

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