C₁₅H₁₈O₄

Base Information

Chemical Name:C₁₅H₁₈O₄
CAS No.:1252651-73-2
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:

C<sub>15</sub>H<sub>18</sub>O<sub>4</sub>

Synonyms:C₁₅H₁₈O₄

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Chemical Property of C₁₅H₁₈O₄

Chemical Property:

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Technology Process of C₁₅H₁₈O₄

There total 7 articles about C₁₅H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1252651-72-1
C₁₅H₂₀O₅

: 1252651-73-2
C₁₅H₁₈O₄

Guidance literature:: C₁₅H₂₀O₅; With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja107190w

Reference yield:

: C₁₆H₁₉F₃O₇S

: 1252651-73-2
C₁₅H₁₈O₄

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja2041964

Reference yield:

: 1252651-63-0
C₁₂H₁₄O₃

: 1252651-73-2
C₁₅H₁₈O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hexacyanoferrate (III); (DHQD)2PHAL; potassium osmate; methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 0 °C / Inert atmosphere

1.2: 0.67 h / 20 °C / Inert atmosphere

2.1: pyridinium p-toluenesulfonate / acetone / 1 h / 20 °C / Inert atmosphere

3.1: pyridine / dichloromethane / -78 - 0 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridine; potassium hexacyanoferrate (III); (DHQD)2PHAL; potassium osmate; methanesulfonamide; pyridinium p-toluenesulfonate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; water; acetone; tert-butyl alcohol; 1.1: Sharpless dihydroxylation;
DOI:10.1021/ja2041964