N-1-phenethylhydroxypivalamide

Base Information

Chemical Name:N-1-phenethylhydroxypivalamide
CAS No.:128037-43-4
Molecular Formula:C₁₃H₁₉NO₂
Molecular Weight:221.299
Hs Code.:

Synonyms:N-1-phenethylhydroxypivalamide

Suppliers and Price of N-1-phenethylhydroxypivalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-1-phenethylhydroxypivalamide

Chemical Property:

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Technology Process of N-1-phenethylhydroxypivalamide

There total 3 articles about N-1-phenethylhydroxypivalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 128037-39-8
Acetic acid 3-[cyclohexanecarbonyl-(1-phenyl-ethyl)-amino]-2,2-dimethyl-3-oxo-propyl ester

: 128037-43-4
N-1-phenethylhydroxypivalamide

: 98-89-5
Cyclohexanecarboxylic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; for 24h; Product distribution; Mechanism; Ambient temperature;
DOI:10.1016/S0040-4039(00)94615-X

Reference yield:

: 58908-50-2
3-acetoxy-2,2-dimethylpropionyl chloride

: 128037-43-4
N-1-phenethylhydroxypivalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Et₃N, 4-N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 8 h / Ambient temperature

2: aq LiOH / tetrahydrofuran / 24 h / Ambient temperature

With dmap; lithium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)94615-X

Reference yield:

: 22164-12-1,61765-19-3
N-benzyl-N-methylcyclohexanecarboxamide

: 128037-43-4
N-1-phenethylhydroxypivalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Et₃N, 4-N,N-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 8 h / Ambient temperature

2: aq LiOH / tetrahydrofuran / 24 h / Ambient temperature

With dmap; lithium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)94615-X