3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

Base Information

Chemical Name:3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide
CAS No.:1215021-55-8
Molecular Formula:C₉H₈F₃NO₅S₂
Molecular Weight:331.293
Hs Code.:

Synonyms:3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

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Chemical Property of 3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

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Technology Process of 3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

There total 2 articles about 3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1039755-99-1
N-(2-(trifluoromethane)benzenesulfonyl)ethanolamine

: 1215021-55-8
3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

Guidance literature:: N-(2-(trifluoromethane)benzenesulfonyl)ethanolamine; With thionyl chloride; In acetonitrile; at -20 ℃;

With pyridine; In acetonitrile; at -20 - 0 ℃;

With sodium periodate; ruthenium(III) chloride trihydrate; In water; acetonitrile; at 0 ℃; for 1h;
DOI:10.1002/anie.200905329

Reference yield:

: C₉H₈F₃NO₄S₂

: 1215021-55-8
3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

Guidance literature:: With sodium periodate; ruthenium(III) trichloride hydrate; In water; acetonitrile; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201203825

Reference yield: 80.0%

: 1215021-55-8
3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide

: 375349-06-7
tert-butyl 2,3-dihydro-1-oxo-1H-indene-2-carboxylate

: 1041024-61-6
(S)-tert-butyl 1-oxo-2-(2-(2-(trifluoromethyl)phenylsulfonamido)ethyl)-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: 3-{[2-(trifluoromethyl)phenyl]sulfonyl}1,2,3-oxathiazolidine 2,2-dioxide; tert-butyl 2,3-dihydro-1-oxo-1H-indene-2-carboxylate; With C₄₅H₄₇N₂O₂⁽¹⁺⁾*Cl^(1-); caesium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; at 0 ℃; for 72h;

With hydrogenchloride; water; In 5,5-dimethyl-1,3-cyclohexadiene; at 0 - 20 ℃; for 0.166667h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.200905329