methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

Base Information

Chemical Name:methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2
CAS No.:679401-28-6
Molecular Formula:C₂₀H₃₂O₆Si
Molecular Weight:398.54
Hs Code.:

Synonyms:methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

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Chemical Property of methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

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Technology Process of methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

There total 1 articles about methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

: methyl 1-O-methyl-3-O-benzyl-D-ribofuranuronate-3,4-d2

: 18162-48-6
tert-butyldimethylsilyl chloride

: 679401-27-5
methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-β-D-ribofuranuronate-3,4-d2

: 679401-28-6
methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

Guidance literature:: With pyridine; silver nitrate; In tetrahydrofuran; for 4h;
DOI:10.1081/NCN-120026632

Reference yield: 72.0%

: 679401-28-6
methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

: 679401-30-0
1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranose-3,4,5,5'-d4

Guidance literature:: With lithium aluminium deuteride; In diethyl ether; at 20 ℃; for 2h;
DOI:10.1081/NCN-120026632

Reference yield:

: 679401-28-6
methyl 1-O-methyl-3-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranuronate-3,4-d2

: 679401-32-2
1-O-methyl-3,5-di-O-benzyl-2-O-t-butyldimethylsilyl-α-D-ribofuranose-3,4,5,5'-d4

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / LiAlD₄ / diethyl ether / 2 h / 20 °C

2: 74 percent / NaH / acetonitrile / 4 h / 20 °C

With lithium aluminium deuteride; sodium hydride; In diethyl ether; acetonitrile;
DOI:10.1081/NCN-120026632