3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine

Base Information

• Chemical Name: 3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine
• CAS No.: 126832-38-0
• Molecular Formula: C₃₉H₅₄N₆O₈Si₂
• Molecular Weight: 791.064

Synonyms:3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine

Chemical Property of 3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine

Chemical Property:

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Technology Process of 3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine

There total 2 articles about 3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane (69304-37-6) + O6-diphenylcarbamoyl-N2-isobutyrylguanosine (126832-37-9) → 3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O6-diphenylcarbamoyl-N2-isobutyrylguanosine (126832-38-0)

Guidance literature:

With pyridine;

DOI:10.1007/BF00597663

Reference yield:

O6-diphenylcarbamoyl-N2,2',3',5'-O-tetraisobutyrylguanosine (126832-42-6) → 3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O6-diphenylcarbamoyl-N2-isobutyrylguanosine (126832-38-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / 2 M NaOH / ethanol; pyridine / 0.12 h / 0 °C

2: 92 percent / pyridine

With pyridine; sodium hydroxide; In pyridine; ethanol;

DOI:10.1007/BF00597663

Reference yield: 42.0%

3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3,diyl)-O6-diphenylcarbamoyl-N2-isobutyrylguanosine (126832-38-0) + methyl iodide (74-88-4) → 2'-O-methyl-O6-diphenylcarbamoyl-N2-isobutyrylguanosine (129496-69-1)

Guidance literature:

With silver(l) oxide; In acetone; at 20 ℃;

DOI:10.1007/BF00597663

upstream raw materials:

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine

O⁶-diphenylcarbamoyl-N²,2',3',5'-O-tetraisobutyrylguanosine

Downstream raw materials:

2'-O-methyl-O⁶-diphenylcarbamoyl-N²-isobutyrylguanosine

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