N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

Base Information

Chemical Name:N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine
CAS No.:106163-21-7
Molecular Formula:C₃₄H₅₄N₄O₆
Molecular Weight:614.826
Hs Code.:

Synonyms:N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

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Chemical Property of N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

Chemical Property:

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Technology Process of N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

There total 5 articles about N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.2%

: 106163-14-8,106163-29-5
Decanedioic acid bis-({4-[3-(benzyl-isopropyl-amino)-2-hydroxy-propoxy]-phenyl}-amide)

: 106163-21-7
N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

Guidance literature:: With acetic acid; palladium on activated charcoal; In methanol; for 20h; Ambient temperature;
DOI:10.1021/jm00387a025

Reference yield:

: 6597-75-7
1-(4-acetamidophenoxy)-2,3-epoxypropane

: 106163-21-7
N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / methanol / 5 h / Heating

2: 82.5 percent / HCl / ethanol / 5 h / Heating

3: 45 percent / triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

4: 41.2 percent / 10percent HOAc / 5percent Pd/C / methanol / 20 h / Ambient temperature

With hydrogenchloride; acetic acid; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1021/jm00387a025

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 106163-21-7
N,N'-bis[4-{2-hydroxy-3-[(1-methyethyl)amino]propoxy}phenyl]decanediamine

Guidance literature:: Multi-step reaction with 5 steps

1: 50 percent / NaOH / H₂O / 16 h / Ambient temperature

2: 89 percent / methanol / 5 h / Heating

3: 82.5 percent / HCl / ethanol / 5 h / Heating

4: 45 percent / triethylamine / CH₂Cl₂ / 3 h / Ambient temperature

5: 41.2 percent / 10percent HOAc / 5percent Pd/C / methanol / 20 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; acetic acid; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water;
DOI:10.1021/jm00387a025