methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

Base Information

Chemical Name:methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate
CAS No.:1185730-51-1
Molecular Formula:C₂₉H₄₂N₄O₁₀
Molecular Weight:606.673
Hs Code.:

Synonyms:methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

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Chemical Property of methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

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Technology Process of methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

There total 4 articles about methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1185730-62-4
6-oxo-6-(prop-2-ynylamino)hexan-1-aminium hydrochloride

: 1185730-61-3
C₂₃H₃₀N₄O₉

: 1185730-51-1
methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja809933h

Reference yield:

: 35444-44-1
methyl adipoyl chloride

: 1185730-51-1
methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6.16 h / 0 - 20 °C / Inert atmosphere

2: dichloromethane / 4 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1185730-50-0
methyl 6-((3-(4,5-dimethoxy-2-nitrophenyl)-3-hydroxypropyl)(methyl)amino)-6-oxohexanoate

: 1185730-51-1
methyl 14-(4,5-dimethoxy-2-nitrophenyl)-17-methyl-5,12,18-trioxo-13-oxa-4,11,17-triazatricos-1-yn-23-oate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 4 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;