methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

Base Information

Chemical Name:methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>
CAS No.:79521-07-6
Molecular Formula:C₂₅H₃₈O₆
Molecular Weight:434.573
Hs Code.:

Synonyms:methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

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Chemical Property of methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

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Technology Process of methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

There total 5 articles about methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 79521-18-9
5,5'-[2-(1-hydroxypropyl)-1,4-phenylenebis(oxy)]bis[2,2-dimethylpentanoic acid]

: 79521-07-6
methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 8h; Heating;
DOI:10.1021/jm00361a015

Reference yield:

: 79520-52-8
5-Bromo-2,2-dimethylpentanoic acid,methyl ester

: 79521-07-6
methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 80 - 85 deg C, 12 - 14 h

2: NaBH₄ / methanol / Ambient temperature

3: 2 N NaOH / methanol

4: 46 percent / p-toluenesulfonic acid / benzene / 8 h / Heating

With sodium hydroxide; sodium tetrahydroborate; sodium hydride; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.1021/jm00361a015

Reference yield:

: 79521-06-5
dimethyl 5,5'-[[2-(1-hydroxypropyl)-1,4-phenylene]bis(oxy)]bis[2,2-dimethylpentanoate]

: 79521-07-6
methyl 5,5'<2-(1-propenyl)-1,4-phenylenebis(oxy)>bis<2,2-dimethylpentanoate>

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N NaOH / methanol

2: 46 percent / p-toluenesulfonic acid / benzene / 8 h / Heating

With sodium hydroxide; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.1021/jm00361a015