1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

Base Information

Chemical Name:1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide
CAS No.:74828-37-8
Molecular Formula:C₂₁H₂₄NO₅*I
Molecular Weight:497.33
Hs Code.:

Synonyms:1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

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Chemical Property of 1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

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Technology Process of 1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

There total 4 articles about 1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1-(3',4'-dimethoxybenzyl)-5-methoxy-6,7-methylenedioxy-3,4-dihydroisoquinoline

: 74-88-4
methyl iodide

: 74828-37-8
1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

Guidance literature:: In methanol; for 1h; Heating;
DOI:10.1021/ja00541a021

Reference yield:

: 2220-19-1
β-<2-methoxy-3,4-methylenedioxy-phenyl>-ethylamine

: 74828-37-8
1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 5 h / 160 °C

2: 3.5 g / phosphorus oxychloride / acetonitrile / 2.5 h / Heating

3: 71 percent / methanol / 1 h / Heating

With trichlorophosphate; In methanol; acetonitrile;
DOI:10.1021/ja00541a021

Reference yield:

: 15964-79-1
methyl (3,4-dimethoxyphenyl)acetate

: 74828-37-8
1-(3',4'-dimethoxybenzyl)-2-methyl-5-methoxy-6,7-methylenesdioxy-3,4-dihydroisoquinolinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 5 h / 160 °C

2: 3.5 g / phosphorus oxychloride / acetonitrile / 2.5 h / Heating

3: 71 percent / methanol / 1 h / Heating

With trichlorophosphate; In methanol; acetonitrile;
DOI:10.1021/ja00541a021