dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane

Base Information

• Chemical Name: dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane
• CAS No.: 612836-13-2
• Molecular Formula: C₂₅H₃₅BO₂Si
• Molecular Weight: 406.448

Synonyms:dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane

Chemical Property of dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane

Chemical Property:

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Technology Process of dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane

There total 2 articles about dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H36BO2Si(1-)*Li(1+) → dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane (612836-13-2)

Guidance literature:

With Allyl acetate; palladium diacetate; tricyclohexylphosphine; In tetrahydrofuran; at 60 ℃; for 1h; Sealed tube;

DOI:10.1002/anie.201811782

Reference yield:

(R)-dimethyl(phenyl)(3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl)silane (1270304-75-0) → dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane (612836-13-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere; Sealed tube

2: palladium diacetate; tricyclohexylphosphine; Allyl acetate / tetrahydrofuran / 1 h / 60 °C / Sealed tube

With Allyl acetate; palladium diacetate; tricyclohexylphosphine; In tetrahydrofuran;

DOI:10.1002/anie.201811782

Reference yield:

dimethylphenyl-[(1S)-1-(2-phenylethyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl]silane (612836-13-2) → 2-[(S)-2-(Dimethyl-phenyl-silanyl)-1-methyl-4-phenyl-butyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:

With triethylamine; toluene-4-sulfonic acid hydrazide; In 1,4-dioxane; for 3h; Heating;

DOI:10.1021/ja0368958

upstream raw materials:

(R)-dimethyl(phenyl)(3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl)silane

Downstream raw materials:

(Z)-1-phenyl-3-pentene

(2R,3S)-3-(Dimethyl-phenyl-silanyl)-5-phenyl-pentan-2-ol

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