2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

Base Information

Chemical Name:2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride
CAS No.:949006-06-8
Molecular Formula:C₂₈H₂₈FN₃O₆
Molecular Weight:521.545
Hs Code.:

Synonyms:2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

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Chemical Property of 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

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Technology Process of 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

There total 2 articles about 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 949006-05-7
2-azido-3,6-di-O-benzyl-2-deoxy-β-D-galactopyranosyl fluoride

: 100-07-2
4-methoxy-benzoyl chloride

: 949006-06-8
2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

Guidance literature:: In pyridine; at 20 ℃; for 6.5h;
DOI:10.1016/j.tet.2007.05.126

Reference yield:

: C₂₃H₂₁O₅N₃F₆

: 949006-06-8
2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine; ethanol / 55.5 h / 20 °C

2: 84 percent / pyridine / 6.5 h / 20 °C

In pyridine; ethanol;
DOI:10.1016/j.tet.2007.05.126

Reference yield: 40.0%

: 904891-28-7
tert-butyldiphenylsilyl 2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

: 949006-06-8
2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-β-D-galactopyranosyl fluoride

: tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(4-methoxybenzoyl)-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

Guidance literature:: With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver perchlorate; In chloroform; at 20 ℃; for 42h;
DOI:10.1016/j.tet.2007.05.126