1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

Base Information

Chemical Name:1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate
CAS No.:1008762-50-2
Molecular Formula:C₁₃H₁₇N₂*C₂₄H₂₀B
Molecular Weight:520.525
Hs Code.:

Synonyms:1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

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Chemical Property of 1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

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Technology Process of 1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

There total 1 articles about 1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 1008762-50-2
1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: dichloromethane / 1 h

In dichloromethane; acetonitrile;
DOI:10.1039/c8cy01214h

Reference yield: 90.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 1008762-50-2
1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

: [Ir(MesIMe)CODCl]

Guidance literature:: 1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate; With potassium carbonate; In acetone; for 0.166667h; Inert atmosphere;

bis(1,5-cyclooctadiene)diiridium(I) dichloride; In acetone; Inert atmosphere; Reflux;
DOI:10.1039/c9dt00313d

Reference yield: 71.0%

: 131296-74-7
Os(hydride)6(triisopropylphosphine)2

: 1008762-50-2
1-methyl-3-(2,4,6-trimethylphenyl)-1H-imidazolium tetraphenylborate

: [OsH₅(1-mesityl-3-methylimidazol-4-ylidene)(P(i-Pr)3)2]BPh₄

Guidance literature:: In tetrahydrofuran; byproducts: H2; Schlenk technique; soln. of Os complex in THF was treated with imidazolium salt (1 equiv.); stirred at 90°C for 5 h; cooled to room temp.; filtered through Celite; solvent removed; Et2O added; washed (Et2O); dried (vac.); elem. anal.;
DOI:10.1021/om7010722