2,4,6-triethylbenzoic acid chloride

Base Information

Chemical Name:2,4,6-triethylbenzoic acid chloride
CAS No.:22019-76-7
Molecular Formula:C₁₃H₁₇ClO
Molecular Weight:224.73
Hs Code.:

Synonyms:2,4,6-triethylbenzoic acid chloride

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Chemical Property of 2,4,6-triethylbenzoic acid chloride

Chemical Property:

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Technology Process of 2,4,6-triethylbenzoic acid chloride

There total 3 articles about 2,4,6-triethylbenzoic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92035-96-6
2,4,6-triethylbenzoic acid

: 22019-76-7
2,4,6-triethylbenzoic acid chloride

Guidance literature:: With thionyl chloride;
DOI:10.1021/ja01877a018

Reference yield:

: 102-25-0
1,3,5-triethylbenzene

: 22019-76-7
2,4,6-triethylbenzoic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 92 percent / Br₂; Fe / CCl₄

2.1: Mg; 1,2-dibromoethane / diethyl ether / 3 h

2.2: 60 percent / diethyl ether / 20 °C

3.1: SOCl₂ / CH₂Cl₂; dimethylformamide / 5.5 h

With thionyl chloride; bromine; iron; magnesium; ethylene dibromide; In tetrachloromethane; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b200358a

Reference yield:

: 91-06-5
2-bromo-1,3,5-triethylbenzene

: 22019-76-7
2,4,6-triethylbenzoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg; 1,2-dibromoethane / diethyl ether / 3 h

1.2: 60 percent / diethyl ether / 20 °C

2.1: SOCl₂ / CH₂Cl₂; dimethylformamide / 5.5 h

With thionyl chloride; magnesium; ethylene dibromide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b200358a