2,4,6-Triethylbenzenethiocarboxylic acid S-(2-hydroxy-2-phenylbutyl) ester

Base Information

• Chemical Name: 2,4,6-Triethylbenzenethiocarboxylic acid S-(2-hydroxy-2-phenylbutyl) ester
• CAS No.: 67902-79-8
• Molecular Formula: C₂₃H₃₀O₂S
• Molecular Weight: 370.556
• Mol file: 67902-79-8.mol

Synonyms:2,4,6-Triethylbenzenethiocarboxylic acid S-(2-hydroxy-2-phenylbutyl) ester

Chemical Property of 2,4,6-Triethylbenzenethiocarboxylic acid S-(2-hydroxy-2-phenylbutyl) ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6-Triethylbenzenethiocarboxylic acid S-(2-hydroxy-2-phenylbutyl) ester

There total 2 articles about 2,4,6-Triethylbenzenethiocarboxylic acid S-(2-hydroxy-2-phenylbutyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-triethylbenzoic acid chloride (22019-76-7) → 2,4,6-Triethyl-thiobenzoic acid S-(2-hydroxy-2-phenyl-butyl) ester (67902-79-8)

Guidance literature:

Multi-step reaction with 2 steps

1: MeSH

2: (i) nBuLi, THF, hexane, (ii) /BRN= 606215/

With methylthiol;

DOI:10.1021/ja00485a030

Reference yield:

Methyl-2,4,6-Triethylthiobenzoat (64712-51-2) + 1-phenyl-propan-1-one (93-55-0) → 2,4,6-Triethyl-thiobenzoic acid S-(2-hydroxy-2-phenyl-butyl) ester (67902-79-8)

Guidance literature:

Multistep reaction; (i) nBuLi, THF, hexane, (ii) /BRN= 606215/;

DOI:10.1021/ja00485a030

upstream raw materials:

Methyl-2,4,6-Triethylthiobenzoat

1-phenyl-propan-1-one

2,4,6-triethylbenzoic acid chloride