1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane
CAS No.:1621595-66-1
Molecular Formula:C₁₆H₂₂B₁₀N₂
Molecular Weight:350.474
Hs Code.:

Synonyms:1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

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Chemical Property of 1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

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Technology Process of 1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

There total 3 articles about 1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1621595-64-9
1-(4-aminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

: 74-88-4
methyl iodide

: 1621595-66-1
1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

: 1621595-68-3
1-(4-cyanophenyl)-2-(4-dimethylaminophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: In N,N-dimethyl-formamide; at 0 - 40 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1621595-66-1
1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

: 1621595-68-3
1-(4-cyanophenyl)-2-(4-dimethylaminophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; tetrahydrofuran / 3 h / 20 °C

3.1: N,N-dimethyl-formamide / 48 h / 0 - 40 °C / Inert atmosphere

With 10 wt% Pd(OH)2 on carbon; hydrogen; sodium hydride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield:

: 1621595-62-7
1-(4-cyanophenyl)-2-(4-nitrophenyl)-1,2-dicarba-closo-dodecaborane

: 1621595-66-1
1-(4-cyanophenyl)-2-(4-methylaminophenyl)-1,2-dicarba-closo-dodecaborane

: 1621595-68-3
1-(4-cyanophenyl)-2-(4-dimethylaminophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: Multi-step reaction with 2 steps

1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; tetrahydrofuran / 3 h / 20 °C

2: N,N-dimethyl-formamide / 48 h / 0 - 40 °C / Inert atmosphere

With 10 wt% Pd(OH)2 on carbon; hydrogen; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.07.034