methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

Base Information

Chemical Name:methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate
CAS No.:1350846-57-9
Molecular Formula:C₁₈H₂₅NO₆
Molecular Weight:351.4
Hs Code.:

Synonyms:methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

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Technology Process of methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

There total 1 articles about methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: C₁₈H₂₅NO₅

: C₁₈H₂₃NO₆

: 1350846-57-9
methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

Guidance literature:: With tert.-butylhydroperoxide; ruthenium(III) trichloride hydrate; In decane; benzene; at 20 ℃; for 7h; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tetasy.2011.09.021

Reference yield: 82.0%

: 1350846-57-9
methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

: 101669-80-1
methyl (3S,4S)-N-tert-butoxycarbonyl-4-amino-3-hydroxy-5-phenylpentanoate

Guidance literature:: With methanol; toluene-4-sulfonic acid; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2011.09.021

Reference yield:

: 1350846-57-9
methyl (3S,4S)-3-O-formyl-4-(tert-butoxycarbonyl)amino-5-phenylpentanoate

: 72155-48-7
(3S,4S)-4-tert-butoxycarbonylamino-3-hydroxy-5-phenylpentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; toluene-4-sulfonic acid / 1 h / 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran / 1 h / 20 °C

2.2: Cooling

With methanol; water; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2011.09.021