S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate

Base Information

• Chemical Name: S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate
• CAS No.: 1465082-64-7
• Molecular Formula: C₁₁H₁₁ClO₃S₂
• Molecular Weight: 290.792
• Mol file: 1465082-64-7.mol

Synonyms:S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate

Chemical Property of S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate

There total 1 articles about S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

chloro-acetic acid-(4-chloro-phenyl ester) (3261-07-2) + potassium ethyl xanthogenate (140-89-6) → S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate (1465082-64-7)

Guidance literature:

In acetone; at 20 ℃; for 2h;

DOI:10.1039/c3ra42932f

Reference yield: 84.0%

allyl methyl sulfone (16215-14-8) + S-[2-(4-chlorophenoxy)-2-oxoethyl] O-ethyl carbonodithioate (1465082-64-7) → S-[1,7-di(4-chlorophenoxy)-1,7-dioxoheptan]-4-yl O-ethyl carbonodithioate (1465082-79-4)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; for 8h; Inert atmosphere; Reflux;

DOI:10.1039/c3ra42932f

upstream raw materials:

chloro-acetic acid-(4-chloro-phenyl ester)

potassium ethyl xanthogenate

Downstream raw materials:

S-[1,7-di(4-chlorophenoxy)-1,7-dioxoheptan]-4-yl O-ethyl carbonodithioate