N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

Base Information

Chemical Name:N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine
CAS No.:105148-64-9
Molecular Formula:C₃₀H₂₉NO₇
Molecular Weight:515.563
Hs Code.:

Synonyms:N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

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Chemical Property of N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

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Technology Process of N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

There total 8 articles about N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,4S)-2-Benzyl-4-(2-benzyloxycarbonyl-ethylcarbamoyl)-5-phenyl-pentanoic acid 3-oxo-1,3-dihydro-isobenzofuran-1-yl ester

: 105148-64-9
N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00132a005

Reference yield:

: 105129-13-3
threo-2,4-dibenzylglutaric acid

: 105148-64-9
N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

Guidance literature:: Multi-step reaction with 7 steps

1: acetyl chloride / toluene / 2 h

2: 15percent Et₃N / toluene / 0.25 h / 50 °C

3: H₂O / dioxane / Heating

4: 98 percent / Ac₂O / toluene / 2 h

5: toluene / Heating

6: N(Et)3, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

7: H₂ / 5percent Pd/C / ethanol / 760 Torr / Ambient temperature

With water; hydrogen; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; acetyl chloride; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane; toluene;
DOI:10.1021/jm00132a005

Reference yield:

: 16859-59-9
3-hydroxy-1(3H)-isobenzofuranone

: 105148-64-9
N-<(S,S)-2,4-dibenzyl-4-<<(1-oxo-2-benzofuran-3-yl)oxy>carbonyl>butyryl>-β-alanine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / Heating

2: N(Et)3, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

3: H₂ / 5percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm00132a005