4-[(3-methoxybenzoyl)amino]benzoic chloride

Base Information

• Chemical Name: 4-[(3-methoxybenzoyl)amino]benzoic chloride
• CAS No.: 1160636-08-7
• Molecular Formula: C₁₅H₁₂ClNO₃
• Molecular Weight: 289.718
• Mol file: 1160636-08-7.mol

Synonyms:4-[(3-methoxybenzoyl)amino]benzoic chloride

Chemical Property of 4-[(3-methoxybenzoyl)amino]benzoic chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-[(3-methoxybenzoyl)amino]benzoic chloride

There total 1 articles about 4-[(3-methoxybenzoyl)amino]benzoic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

4-[(3-methoxybenzoyl)amino]benzoic acid (97394-52-0) → 4-[(3-methoxybenzoyl)amino]benzoic chloride (1160636-08-7)

Guidance literature:

With thionyl chloride; In dichloromethane; for 1h; Reflux;

DOI:10.1039/b901898k

Reference yield: 15.0%

4-[(3-methoxybenzoyl)amino]benzoic chloride (1160636-08-7) + 1-methyl-4-[(E)-2-(1-methyl-4-nitro-1H-pyrrol-2-yl)ethenyl]-N-[2-(4-morpholinyl)ethyl]-1H-pyrrole-2-carboxamide (1160636-07-6) + trifluoroacetic acid (76-05-1) → 4-{(E)-2-[4-({4-[(3-methoxybenzoyl)amino]benzoyl}amino)-1-methyl-1H-pyrrol-2-yl]ethenyl}-1-methyl-N-[2-(4-morpholinyl)ethyl]-1H-pyrrole-2-carboxamide trifluoroacetate (1160636-00-9) + 4-{2-[4-({4-[(3-methoxybenzoyl)amino]benzoyl}amino)-1-methyl-1H-pyrrol-2-yl]ethyl}-1-methyl-N-[2-(4-morpholinyl)ethyl]-1H-pyrrole-2-carboxamide trifluoroacetate (1160636-02-1)

Guidance literature:

1-methyl-4-[(E)-2-(1-methyl-4-nitro-1H-pyrrol-2-yl)ethenyl]-N-[2-(4-morpholinyl)ethyl]-1H-pyrrole-2-carboxamide; With sodium tetrahydroborate; palladium 10% on activated carbon; In 1,4-dioxane; water;

4-[(3-methoxybenzoyl)amino]benzoic chloride; With sodium carbonate; In 1,4-dioxane; water;

trifluoroacetic acid; With silica gel; In water;

DOI:10.1039/b901898k

upstream raw materials:

4-[(3-methoxybenzoyl)amino]benzoic acid

Downstream raw materials:

4-{(E)-2-[4-({4-[(3-methoxybenzoyl)amino]benzoyl}amino)-1-methyl-1H-pyrrol-2-yl]ethenyl}-1-methyl-N-[2-(4-morpholinyl)ethyl]-1H-pyrrole-2-carboxamide trifluoroacetate

4-{2-[4-({4-[(3-methoxybenzoyl)amino]benzoyl}amino)-1-methyl-1H-pyrrol-2-yl]ethyl}-1-methyl-N-[2-(4-morpholinyl)ethyl]-1H-pyrrole-2-carboxamide trifluoroacetate