cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

Base Information

Chemical Name:cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine
CAS No.:179173-99-0
Molecular Formula:C₂₈H₂₉N₅O
Molecular Weight:451.571
Hs Code.:

Synonyms:cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

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Chemical Property of cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

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Technology Process of cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

There total 6 articles about cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1144-74-7
4-nitrobenzophenone

: 179173-99-0
cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / tetrahydrofuran / 0.75 h

1.2: tetrahydrofuran / 18 h / Heating

2.1: aq. K₂CO₃ / methanol / 4 h / Heating

3.1: HOBt; DCC / dimethylformamide / 18 h / 20 °C

4.1: H₂ / 10percent Pd/C / methanol / 18 h

With hydrogen; sodium hydride; potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; 10percent Pd/C; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm010852p

Reference yield:

: 17683-99-7
E/Z-3-(4-nitrophenyl)-3-phenylpropenoic acid

: 179173-99-0
cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: HOBt; DCC / dimethylformamide / 18 h / 20 °C

2: H₂ / 10percent Pd/C / methanol / 18 h

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; 10percent Pd/C; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm010852p

Reference yield:

: 21320-81-0
ethyl 3-(4-nitrophenyl)-3-phenylacrylate

: 179173-99-0
cis-1-[[1-[3-(4-Aminophenyl)-3-phenylpropenoyl]-4-piperidyl]methyl]-1H-2-methylimidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: aq. K₂CO₃ / methanol / 4 h / Heating

2: HOBt; DCC / dimethylformamide / 18 h / 20 °C

3: H₂ / 10percent Pd/C / methanol / 18 h

With hydrogen; potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; 10percent Pd/C; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm010852p