Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI)
CAS No.:153833-65-9
Molecular Formula:C₁₀H₁₇NO₂
Molecular Weight:183.25
Hs Code.:
Mol file:153833-65-9.mol

Synonyms:Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(R)-tert-Butylcyclopent-2-en-1-ylcarbamate 95+%
1g
$ 1501.00

Total 1 raw suppliers

Chemical Property of Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

PSA：41.82000
LogP:2.43410

Purity/Quality:: (R)-tert-Butylcyclopent-2-en-1-ylcarbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI)

There total 12 articles about Carbamic acid, (1R)-2-cyclopenten-1-yl-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 81097-48-5
N-tosyl-6-azabicyclo[3.1.0]hexane

: 70-55-3
toluene-4-sulfonamide

: 153833-65-9,156731-34-9
(1R)-1-(tert-butoxycarbonylamino)cyclopenta-2-ene

: 153833-65-9,156731-34-9
tert-butyl (1S)-2-cyclopenten-1-ylcarbamate

Guidance literature:: N-tosyl-6-azabicyclo[3.1.0]hexane; With sec.-butyllithium; (-)-sparteine; In diethyl ether; cyclohexane; at -78 ℃; for 4h;

di-tert-butyl dicarbonate; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h;

With ammonia; sodium; In tetrahydrofuran; at -78 - 20 ℃; Title compound not separated from byproducts;
DOI:10.1016/j.tet.2003.09.024

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 81097-48-5
N-tosyl-6-azabicyclo[3.1.0]hexane

: 70-55-3
toluene-4-sulfonamide

: 153833-65-9,156731-34-9
(1R)-1-(tert-butoxycarbonylamino)cyclopenta-2-ene

: 153833-65-9,156731-34-9
tert-butyl (1S)-2-cyclopenten-1-ylcarbamate

Guidance literature:: N-tosyl-6-azabicyclo[3.1.0]hexane; With sec.-butyllithium; (-)-sparteine; In diethyl ether; cyclohexane; at -78 ℃; for 4h;

di-tert-butyl dicarbonate; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h;

With ammonia; sodium; In tetrahydrofuran; at -78 - 20 ℃; Title compound not separated from byproducts;
DOI:10.1016/j.tet.2003.09.024

Reference yield:

: 100727-30-8
2-(cyclopent-2-en-1-yl)isoindoline-1,3-dione

: 24424-99-5
di-tert-butyl dicarbonate

: 144019-33-0,153833-65-9,156731-34-9
tert-butyl cyclopent-2-ene-1-carbamate

Guidance literature:: 2-(cyclopent-2-en-1-yl)isoindoline-1,3-dione; With hydrazine hydrate; In water; at 70 ℃; for 2h;

di-tert-butyl dicarbonate; In water; at 20 ℃;