4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine

Base Information

• Chemical Name: 4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine
• CAS No.: 1046144-93-7
• Molecular Formula: C₂₉H₄₆N₄O₃Si
• Molecular Weight: 526.795
• Mol file: 1046144-93-7.mol

Synonyms:4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine

Chemical Property of 4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine

There total 1 articles about 4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,6-di-n-butyrylamino-4-iodo-pyridine (1046144-90-4) + tris[4-(N-tert-butyl-N-[tert-butyldimethylsiloxyl]amino)phenyl]boroxin (371248-60-1) → 4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine (1046144-93-7)

Guidance literature:

2,6-di-n-butyrylamino-4-iodo-pyridine; With palladium diacetate; In tetrahydrofuran; for 0.0833333h;

tris[4-(N-tert-butyl-N-[tert-butyldimethylsiloxyl]amino)phenyl]boroxin; With potassium carbonate; In tetrahydrofuran; water; Reflux; Inert atmosphere;

DOI:10.1039/b800779a

Reference yield: 70.0%

4-(4'-[N-tert-butyl-N-(tert-butyldimethylsiloxyl)amino])-2,6-di-n-butyrylaminopyridine (1046144-93-7) → 4-(4'-[N-tert-butyl-N-hydroxylamino])-2,6-di-n-butyrylaminopyridine (1046144-94-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1039/b800779a

upstream raw materials:

2,6-di-n-butyrylamino-4-iodo-pyridine

tris[4-(N-tert-butyl-N-[tert-butyldimethylsiloxyl]amino)phenyl]boroxin

Downstream raw materials:

4-(4'-[N-tert-butyl-N-hydroxylamino])-2,6-di-n-butyrylaminopyridine