ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate

Base Information

• Chemical Name: ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate
• CAS No.: 207286-87-1
• Molecular Formula: C₂₂H₂₇BrNO₆P
• Molecular Weight: 512.337

Synonyms:ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate

Chemical Property of ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate

Chemical Property:

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Technology Process of ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate

There total 1 articles about ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinic acid (108327-37-3) + ethyl 4-bromo-α-methylenebenzenepropanoate (207286-80-4) → ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate (207286-87-1)

Guidance literature:

With N,O-bis-(trimethylsilyl)-acetamide;

DOI:10.1021/jm990483l

Reference yield: 98.0%

ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate (207286-87-1) → 3-[(1-benzyloxycarbonylamino-ethyl)-hydroxy-phosphinoyl]-2-(4-bromo-benzyl)-propionic acid (268225-10-1)

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃;

DOI:10.1021/jm990483l

Reference yield: 97.6%

ethyl 3-(4-bromophenyl)-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate (207286-87-1) + phenylboronic acid (98-80-6) → Ethyl 3-[1,1'-biphenyl]-4-yl-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate (207286-88-2)

Guidance literature:

upstream raw materials:

[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinic acid

ethyl 4-bromo-α-methylenebenzenepropanoate

Downstream raw materials:

3-[(1-benzyloxycarbonylamino-ethyl)-hydroxy-phosphinoyl]-2-(4-bromo-benzyl)-propionic acid

Ethyl 3-[1,1'-biphenyl]-4-yl-2-[[hydroxy[1-[[(phenylmethoxy)carbonyl]amino]ethyl]phosphinyl]methyl]propanoate

2-[(1-Benzyloxycarbonylamino-ethyl)-hydroxy-phosphinoylmethyl]-3-biphenyl-4-yl-propionic acid

(S)-2-{3-[(1-Benzyloxycarbonylamino-ethyl)-hydroxy-phosphinoyl]-2-biphenyl-4-ylmethyl-propionylamino}-3-phenyl-propionic acid

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