diphenylphosphinobenzyl-2-methylthioether

Base Information

Chemical Name:diphenylphosphinobenzyl-2-methylthioether
CAS No.:75637-68-2
Molecular Formula:C₂₀H₁₉PS
Molecular Weight:322.411
Hs Code.:

Synonyms:diphenylphosphinobenzyl-2-methylthioether

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Chemical Property of diphenylphosphinobenzyl-2-methylthioether

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Technology Process of diphenylphosphinobenzyl-2-methylthioether

There total 3 articles about diphenylphosphinobenzyl-2-methylthioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: (2-ethylsulfanyl-benzyl)-trimethyl-ammonium; iodide

: 829-85-6
diphenylphosphane

: 75637-68-2
diphenylphosphinobenzyl-2-methylthioether

Guidance literature:: diphenylphosphane; With sodium; In tetrahydrofuran; at 20 ℃;

(2-ethylsulfanyl-benzyl)-trimethyl-ammonium; iodide; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/b502195b

Reference yield: 45.0%

: 2-methyl-mercaptobenzyl-trimethylammonium iodide

: 4376-01-6
sodium diphenylphosphide

: 75637-68-2
diphenylphosphinobenzyl-2-methylthioether

Guidance literature:: In tetrahydrofuran; Ambient temperature;

Reference yield:

: 74484-52-9
dimethyl[(2-methylsulfanyl)benzyl]amine

: 75637-68-2
diphenylphosphinobenzyl-2-methylthioether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1.04 g / acetonitrile / 20 °C

2.1: Na / tetrahydrofuran / 20 °C

2.2: 52 percent / tetrahydrofuran / 20 °C

With sodium; In tetrahydrofuran; acetonitrile;
DOI:10.1039/b502195b