Technology Process of C17H28N4O3
There total 6 articles about C17H28N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
In
ethyl acetate;
under 2585.81 Torr;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C
2.1: caesium carbonate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / N,N-dimethyl-formamide / 110 °C
3.1: hydrogenchloride / 1,4-dioxane; water / 2 h / 70 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere
4.2: 2 h / 50 °C / Reflux
5.1: hydrogen / ethyl acetate / 2585.81 Torr
With
hydrogenchloride; hydrogen; sodium hydride; potassium carbonate; caesium carbonate;
palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
tetrahydrofuran; 1,4-dioxane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C
2.1: caesium carbonate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / N,N-dimethyl-formamide / 110 °C
3.1: hydrogenchloride / 1,4-dioxane; water / 2 h / 70 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere
4.2: 2 h / 50 °C / Reflux
5.1: hydrogen / ethyl acetate / 2585.81 Torr
With
hydrogenchloride; hydrogen; sodium hydride; potassium carbonate; caesium carbonate;
palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
tetrahydrofuran; 1,4-dioxane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;