<5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside

Base Information

• Chemical Name: <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside
• CAS No.: 223906-62-5
• Molecular Formula: C₃₁H₃₀O₈
• Molecular Weight: 531.563
• Mol file: 223906-62-5.mol

Synonyms:<5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside

Chemical Property of <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside

There total 4 articles about <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

benzoyl chloride (98-88-4) + [5'-13C]pent-4-enyl D-erythropentofuranoside → <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside (223906-62-5) + [5'-13C]pent-4-enyl 2;,3',5'-tri-O-benzoyl-α-D-erythropentofuranoside (288851-18-3)

Guidance literature:

With pyridine; at 20 ℃; for 24h;

DOI:10.1002/1099-1344(200006)43:7<635::AID-JLCR348>3.0.CO;2-C

Reference yield:

n-Pent-4-enyl alcohol (821-09-0) → <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside (223906-62-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CSA / Ambient temperature

2: pyridine

With camphor-10-sulfonic acid; In pyridine;

DOI:10.1080/00397919908086048

Reference yield:

<5-13C>D-ribose → <5'-13C>pent-4-enyl 2',3',5'-tri-O-benzoyl-β-D-erythro-pentofuranoside (223906-62-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CSA / Ambient temperature

2: pyridine

With camphor-10-sulfonic acid; In pyridine;

DOI:10.1080/00397919908086048

upstream raw materials:

benzoyl chloride

n-Pent-4-enyl alcohol

Downstream raw materials:

N⁶,O^2',O^3',O^5'-tetrabenzoyl[5'-13C]adenosine

[5'-13C]adenosine