Re₂Os*13CO*CH₃CN=Re₂Os(CO)13(CH₃CN)

Base Information

• Chemical Name: Re₂Os*13CO*CH₃CN=Re₂Os(CO)13(CH₃CN)
• CAS No.: 98688-93-8
• Molecular Formula: 13CO*C₂H₃N*OsRe₂
• Molecular Weight: 967.802

Synonyms:Re₂Os*13CO*CH₃CN=Re₂Os(CO)13(CH₃CN)

Chemical Property of Re₂Os*13CO*CH₃CN=Re₂Os(CO)13(CH₃CN)

Chemical Property:

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Technology Process of Re₂Os*13CO*CH₃CN=Re₂Os(CO)13(CH₃CN)

There total 1 articles about Re₂Os*13CO*CH₃CN=Re₂Os(CO)13(CH₃CN) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydridopentacarbonylrhenium(I) (16457-30-0) + (CO)4Os(CH2CH3)2 → Re2Os*13CO*CH3CN=Re2Os(CO)13(CH3CN) (98688-93-8) + propionaldehyde (123-38-6)

Guidance literature:

With CH₃CN; In acetonitrile; byproducts: C2H6; Et2Os(CO)4 and HRe(CO)5 (in 1:2 molar ratio) were heated in MeCN at 50°C for 30 h; solvent was removed in vacuo, residue washed with hexane, dissolved in CH2Cl2, Re2Os(CO)13(MeCN) was pptd. with hexane;

upstream raw materials:

hydridopentacarbonylrhenium(I)

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