2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

Base Information

Chemical Name:2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane
CAS No.:205994-51-0
Molecular Formula:C₁₆H₃₃BrOSi₄
Molecular Weight:433.683
Hs Code.:

Synonyms:2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

Chemical Property:

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Technology Process of 2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

There total 2 articles about 2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18982-54-2
o-bromobenzyl alcohol

: 5565-32-2
chlorotris(trimethylsilyl)silane

: 205994-51-0
2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 0.5h; Ambient temperature;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<759::AID-CHEM759>3.0.CO;2-V

Reference yield:

: 1873-77-4
tris-(trimethylsilyl)silane

: 205994-51-0
2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

Guidance literature:: Multi-step reaction with 2 steps

1: CCl₄ / 12 h

2: 87 percent / imidazole / dimethylformamide / 0.5 h / Ambient temperature

With 1H-imidazole; tetrachloromethane; In N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<759::AID-CHEM759>3.0.CO;2-V

Reference yield:

: 205994-51-0
2-[(2-bromobenzyl)oxy]-1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)trisilane

: 1,1-bis(trimethylsilyl)-1,3-dihydrobenzo[c][1,2]oxasilole

: 205994-56-5
1-[tris(trimethylsilyl)silyl]benzyl alcohol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;
DOI:10.1002/(SICI)1521-3773(19980302)37:4<462::AID-ANIE462>3.0.CO;2-M