Benzoic acid, 4-[(aminoacetyl)amino]-, methyl ester (9CI)

Base Information

Chemical Name:Benzoic acid, 4-[(aminoacetyl)amino]-, methyl ester (9CI)
CAS No.:153720-00-4
Molecular Formula:C10H12 N2 O3
Molecular Weight:208.217
Hs Code.:
Mol file:153720-00-4.mol

Synonyms:Benzoicacid, 4-[(aminoacetyl)amino]-, methyl ester (9CI);4-(2-Aminoacetylamino)benzoic acid methyl ester

Suppliers and Price of Benzoic acid, 4-[(aminoacetyl)amino]-, methyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
methyl4-(glycylamino)benzoate
100mg
$ 265.00

Crysdot
Methyl4-(2-aminoacetamido)benzoate 95+%
10g
$ 942.00

AK Scientific
methyl4-(glycylamino)benzoate
100mg
$ 179.00

AK Scientific
methyl4-(glycylamino)benzoate
50mg
$ 129.00

Total 2 raw suppliers

Chemical Property of Benzoic acid, 4-[(aminoacetyl)amino]-, methyl ester (9CI)

Chemical Property:

PSA：81.42000
LogP:1.14370

Purity/Quality:

99% ^*data from raw suppliers

methyl4-(glycylamino)benzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-[(aminoacetyl)amino]-, methyl ester (9CI)

There total 5 articles about Benzoic acid, 4-[(aminoacetyl)amino]-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 250789-96-9
methyl 4-{[(tertbutoxycarbonylamino)acetyl]amino}benzoate

: 153720-00-4
methyl 4-[(aminoacetyl)amino]benzoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmcl.2007.06.029

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 153720-00-4
methyl 4-[(aminoacetyl)amino]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / BOP; DIEA / dimethylformamide / 1.5 h / 20 °C

2: 100 percent / TFA / CH₂Cl₂ / 1.5 h / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.06.029